I am on TestCip 250mg a week. Got some raw powers from to make my own batch. Well everything looked good following the cooking recipe but after about an hour it turned into a coagulated mess in the vial. 5grms down the drain. I am looking for any feed back on anyone that may have had success making Test Cip. Could use some help

Now I am an old fart, so trying to remember back to high school chem, so it was probably my error. I have another 10grms but dont know if I should attempt again.
I have read and followed the recepie but to no avail.